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Modification of HVOF and cold spray deposited coatings via electron beam technology
Vacek, Petr ; Šiška, Filip (referee) ; Čížek, Jan (advisor)
The aim of this thesis was to modify microstructure and coating-substrate interface of CoNiCrAlY coatings deposited by HVOF and cold spray on Inconel 718 substrates. Electron beam remelting and annealing in a protective atmosphere were used to modify the coatings. Microstructure, chemical and phase composition were analyzed. The effect of beam current, transversal velocity and beam defocus on remelted depth was evaluated. As-sprayed microstructure and chemical composition of coatings were analyzed and compared with remelted samples. The effect of annealing of the as-sprayed and remelted samples was evaluated. Remelted layers exhibited dendritic structure. Chemical composition changed only after remelting of interface and part of a substrate. When only the coating was remelted, chemical composition remained the same. Phases coarsened after the annealing. Chemical composition changed after annealing due to the diffusion.
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Study of the Ta2O5 insulating layer degradation
Velísek, Martin ; Majzner, Jiří (referee) ; Sedláková, Vlasta (advisor)
The aim of the thesis is to examine the dielectric function Ta2O5 insulating layers in tantalum capacitors. The capacitor plugged in the regular mode represents a MIS structure of reverse direction. Three different factors can be determined for the residual current of the component according to its charge transmission mode: the ohmic, Pool–Frenkel, tunnel and Schottky. An apparatus was constructed by the author of the thesis to measure the temporary connection between residual current and rise of temperature of the tantalum capacitors. Annealing of three different sets of tantalum capacitors made by different producers was performed at the temperature of 400 K and nominal voltage of 35 V during the period of 20 days.The experiment has proved the residual current in the electric field changes with rising temperature in time as a result of the ion movement. The singular factors of the residual current are influenced during the process. By the “ion movement” is meant the ion drift influenced by the attached electric field and diffusion caused by the concentration gradient. First, the samples were being annealed for c. 2 x 106 s, and then the residual current was being regenerated under the voltage of 5 V for 106 s. The residual current values increased considerably after annealing, and decreased again to more or less the original level after the regeneration, some of the samples reaching even values bellow the original level. The VA characteristics of the samples measured before and after the process of controlled obsolescence, and after the regeneration prove not only a change in parameters of the different current factors, but also a change of the current transmission mechanism employed in the process.
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The Study of Productions Operation Management
Petřek, Martin ; Kouřil, Karel (referee) ; Jurová, Marie (advisor)
The thesis dwells about methodics of processing an order in the company: Hardening shop Frydrych s.r.o. while respecting all the demands on the technological process of thermal and thermo-chemical manipulation as annealing, tempering and cementing. On the bases of the analyse and documental procedures the thesis is unraveling a concept for elimination of absences in the sphere of processing the order also as booking, invoicing and evaluating.
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Influence of thermal processing to microstructure of various steels
Kocman, Lukáš ; Havlík, Petr (referee) ; Štěpánek, Roman (advisor)
This bachelor thesis deals with the heat treatment of steel, especially measuring the influence of individual heat treatment technologies on changes in the microstructure of steels. The theoretical part of the work presents alloys of iron and carbon, furthermore describes their phase transformations in the solid state, particularly the transformation diagrams of steels. In another part of theoretical part, the basic heat treatment technologies and their influence on the mechanical properties and microstructure of steels are described. The experimental part deals with the preparation of metallographic samples and presents results of examining the microstructure and measuring the hardness of individual samples. At the end of the work the synthesis of the theoretical part and results of the experimental part is used for the partial and overall evaluation of the influence of heat treatment on the microstructure of steels.
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Analysis of locally modified surfaces for selective growth of cobalt
Krajňák, Tomáš ; Bábor, Petr (referee) ; Čechal, Jan (advisor)
In this thesis the chemical composition of silicon substrates locally modified by focused gallium ion beam by X-ray photoelectron spectroscopy is determined. In order to determine the influence of focused ion beam, the sample comprising sputtered square areas with nominal depths in range of 1 to 10 nm was prepared. Next, the sample was heated to elevated temperatures (500 - 700 °C) to reveal changes in the sputtered areas induced by annealing. In this work by X-ray photoelectron spectrometer Kratos Supra and electron microscope Tescan LYRA3 with focused ion beam were used. From the measured spectra of the Si 2p and Ga 2p3/2 peaks measured as a function of nominal sputtering depth and annealing temperature the following main observations were obtained. First, there is the additional peak component in the Si 2p peak, which can be assigned to the amorphous silicon. The second important finding is that gallium can be removed from near surface volume by annealing at temperatures beyond 700 °C.
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Optimization of thin films of metal oxide materials
Vítek, Jiří ; Šimonová, Lucie (referee) ; Šubarda, Jiří (advisor)
This thesis is focused on the description of the method of reactive sputtering of thin films. Currently, there are many ways how to create thin films and there are many applications of thin films in various industrial sectors. In this paper at the first are listed the issue of thin films, followed by an overview of the deposition techniques and of the chemical analysis of deposited thin films. It also describes the four-point measurement method of sheet resistance, mechanical test of adhesion and optical properties. At the end of the theoretical part are described the material composition of the deposited films. The goal of the practical part is to optimize the deposition process of the mixed layer of indium tin oxide (In2O3: SnO2) and contribute to the overall understanding of the influence of annealing on the layer. There were created six series of samples with that applied layers. First, the work focused on examining of the influence of annealing on the throughput in the whole measuring range, and then comparing the series due to the transmittance in the visible light spectrum. Furthermore were compared the value of sheet resistance of unannealed and subsequently annealed samples.
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Heat treatment of aluminum alloys
Adami, Martin ; Čupera, Jan (referee) ; Němec, Karel (advisor)
This bachelor theses deals with description aluminium alloys, theirs applications in engineering and theirs heat treatment. First part is focused on pure aluminium and its production. The other one is about distribution aluminium alloys by possibility of precipitation hardening.
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Design of flat pallet for automatic parking garage
Osmík, Jiří ; Mrňa, Libor (referee) ; Kubíček, Jaroslav (advisor)
Design of flat pallet for automatic parking garage. Parking and description of automatic parking systems. Welding and weldability of materials. Electric arc welding and welding by melting electrode in protective gas by MIG/MAG method, welding instruments. Design of parking palette calculation and calculation this palette by MKP method. Process of drawing documentation for parking palette. Design of welding process and WPS. Description of annealing and zinc coating. Economic-technical analysis of palette for automatic parking system production.
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